Lead is quantitatively retained on 2-(5-bromo-2-pyridylazo)-5-diethylaminophenol (5-Br-PADAP)-ammonium tetraphenylborate with microcrystalline naphthalene or by a column method in the pH range 4.0-6.0 from a large volume of aqueous solutions of various samples with preconcentration factor of 60. After filtration, the solid mass consisting of the lead complex and naphthalene was dissolved with 5 mL of dimethylformamide and the metal was determined by atomic absorption spectrometry. The calibration curve is linear in the range of 1.9-180 mg/mL in DMF with a relative standard deviation 1.7&. The interference of a large number of anions and cations has been studied.
Taher, M. A. (2001). Atomic Absorption Spectrometric Determination of Lead after Extraction and Preconcentration with 5-Br-PADAP. Iranian Journal of Chemistry and Chemical Engineering, 20(1), 1-8. doi: 10.30492/ijcce.2001.9978
MLA
Mohammad Ali Taher. "Atomic Absorption Spectrometric Determination of Lead after Extraction and Preconcentration with 5-Br-PADAP". Iranian Journal of Chemistry and Chemical Engineering, 20, 1, 2001, 1-8. doi: 10.30492/ijcce.2001.9978
HARVARD
Taher, M. A. (2001). 'Atomic Absorption Spectrometric Determination of Lead after Extraction and Preconcentration with 5-Br-PADAP', Iranian Journal of Chemistry and Chemical Engineering, 20(1), pp. 1-8. doi: 10.30492/ijcce.2001.9978
VANCOUVER
Taher, M. A. Atomic Absorption Spectrometric Determination of Lead after Extraction and Preconcentration with 5-Br-PADAP. Iranian Journal of Chemistry and Chemical Engineering, 2001; 20(1): 1-8. doi: 10.30492/ijcce.2001.9978